Equipment NMR Laboratory

Bruker Avance DRX 500 NMR Spectrometer

Magnet and Spectrometer Console
Superconducting SB magnet, 11.7 T (1H operating frequency 500 MHz)
Spectrometer Console: Two RF channels, digital 2H lock,  BOSS II shim system, z-gradient
Data system: Windows XP,  Topspin 1.3

HPLC-NMR Coupling Options

LC-SPE-MS-NMR
TCI 5 mm Cryoprobe,
Cryo-fit flow systems (30 µl or 60 µl flow cells),
Bruker Esquire 3000 Ion Trap Mass Spectrometer,
Bruker NMR-MS Interface,
Agilent 1100 with autosampler and J&M diode array detector,
BRUKER/SPARK Holland SPE System,
BRUKER Hystar Software.

Bruker Avance 400 NMR Spectrometer

High Resolution NMR
The following probes are available for HR NMR of liquid samples:

• BBO 5 mm: 31P-15N observe, 1H decoupling, automatic tuning and matching (ATM),
• BBI 5mm: 1H observe, 31P-109Ag BB decoupling, ATM, z-gradient
• SEF 3 mm: 19F selective
• SEF 10 mm: 19F selective

Data system: Windows XP, Topspin 2.1

Magnetic Resonance Imaging (MRI)
BRUKER Micro5 imaging probe, modular design by exchangeable rf-inserts:

• 2 mm insert, solenoid coil, 1H selective
• 5 mm insert, 1H selective
• 10 mm insert, tunable to 1H and 19F frequencies

Data system: Linux, ParaVision 2.1.1.