Equipment NMR Laboratory

Bruker Avance III HD 700 NMR Spectrometer

Magnet and Spectrometer Hardware
AscendTM magnet, 16.4 T (1H operating frequency 700 MHz).
Avance III HD spectrometer console.
Probe: TCI  H-C/N-D 1. 7 mm microcryoprobe; ATM.
Autosampler: Sample case. 

Bruker Avance III HD 500 NMR Spectrometer

Magnet and Spectrometer Hardware
UltraShieldPlusTM magnet, 11.7 T (1H operating frequency 500 MHz).
Avance III HD spectrometer console.
Probe: TCI  H-C/N-D 5 mm cryoprobe, ATM.
Autosampler: Sample case.

LC-SPE-MS-NMR Coupling
The TCI 5 mm cryoprobe can be equipped with a CryoFitTM flow insert 
(cell volume 30 µl or 60 µl) for LC-DAD-SPE-NMR coupling. 
LC-DAD: Agilent 1100 with autosampler and J&M diode array detector.
SPE: Bruker/Spark Holland SPE System.
LC-MS: Bruker Esquire 3000 Ion Trap Mass Spectrometer.


Bruker Avance III HD 400 NMR Spectrometer

Magnet and Spectrometer Hardware
UltraShieldTM magnet, 9.4 T (1H operating frequency 400 MHz).
Avance III HD spectrometer console.   
Autosampler: BACS 60.

Liquid State NMR
In the standard configuration, the Avance III HD 400 spectrometer is used for high resolution liquid state NMR. The instrument is operated in full automation with a BACS 60 autosampler, ATM and ICONNMR software.
Standard probe:

  • BBFO 5 mm probe: 31P-19F observe, 1H decoupling, ATM, z-gradient. 

The following probes are optionally available for HR NMR of liquid samples:

  • BBI 5mm: 1H observe, 31P-109Ag BB decoupling, ATM, z-gradient.
  • SEF 3 mm: 19F selective probe.
  • SEF 10 mm: 19F selective probe..


High Resolution Magic Angle Spinning (HR-MAS)

Pneumatic HR-MAS unit.
1H/13C HR MAS probe, 4 mm, MAS gradient.